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Aims.This study explores the metal enrichment signatures attributed to the first generation of stars (Pop III) in the Universe, focusing on the E-XQR-30 sample – a collection of 42 high signal-to-noise ratio spectra of quasi-stellar objects (QSOs) with emission redshifts ranging from 5.8 to 6.6. We aim to identify traces of Pop III metal enrichment by analyzing neutral gas in the interstellar medium of primordial galaxies and their satellite clumps, detected in absorption. Methods.To chase the chemical signature of Pop III stars, we studied metal absorption systems in the E-XQR-30 sample, selected through the detection of the neutral oxygen absorption line at 1302 Å. The O Iline is a reliable tracer of neutral hydrogen and allowed us to overcome the challenges posed by the Lyman-αforest’s increasing saturation at redshifts above ∼5 to identify damped Lyman-αsystems (DLAs). We detected and analyzed 29 O Isystems atz ≥ 5.4, differentiating between proximate DLAs (PDLAs) and intervening DLAs. Voigt function fits were applied to obtain ionic column densities, and relative chemical abundances were determined for 28 systems. These were then compared with the predictions of theoretical models. Results.Our findings expand the study of O Isystems atz ≥ 5.4 fourfold. No systematic differences were observed in the average chemical abundances between PDLAs and intervening DLAs. The chemical abundances in our sample align with literature systems atz >  4.5, suggesting a similar enrichment pattern for this class of absorption systems. A comparison between these DLA-analogs at 4.5 <  z <  6.5 with a sample of very metal-poor DLAs at 2 <  z <  4.5 shows in general similar average values for the relative abundances, with the exception of [C/O], [Si/Fe] and [Si/O] which are significantly larger for the high-zsample. Furthermore, the dispersion of the measurements significantly increases in the high-redshift bin. This increase is predicted by the theoretical models and indicates a potential retention of Pop III signatures in the probed gas. Conclusions.This work represents a significant advancement in the study of the chemical properties of highly neutral gas atz ≥ 5.4, shedding light on its potential association with the metal enrichment from Pop III stars. Future advancements in observational capabilities, specifically high-resolution spectrographs, are crucial for refining measurements and addressing current limitations in the study of these distant absorption systems. 

ABSTRACT Intervening metal absorbers in quasar spectra at z > 6 can be used as probes to study the chemical enrichment of the Universe during the Epoch of Reionization. This work presents the comoving line densities (dn/dX) of low-ionization absorbers, namely, Mg ii (2796 Å), C ii (1334 Å), and O  i (1302 Å) across 2 < z < 6 using the E-XQR-30 metal absorber catalogue prepared from 42 XSHOOTER quasar spectra at 5.8 < z < 6.6. Here, we analyse 280 Mg ii (1.9 < z < 6.4), 22 C ii (5.2 < z < 6.4), and 10 O i (5.3 < z < 6.4) intervening absorbers, thereby building up on previous studies with improved sensitivity of 50 per cent completeness at an equivalent width of W > 0.03 Å. For the first time, we present the comoving line densities of 131 weak (W < 0.3 Å) intervening Mg ii absorbers at 1.9 < z < 6.4 which exhibit constant evolution with redshift similar to medium (0.3 < W < 1.0 Å) absorbers. However, the cosmic mass density of Mg ii – dominated by strong Mg ii systems – traces the evolution of global star formation history from redshift 1.9 to 5.5. E-XQR-30 also increases the absorption path-length by a factor of 50 per cent for C ii and O i whose line densities show a rising trend towards z > 5, in agreement with previous works. In the context of a decline in the metal enrichment of the Universe at z > 5, the overall evolution in the incidence rates of absorption systems can be explained by a weak – possibly soft fluctuating – ultraviolet background. Our results, thereby, provide evidence for a late reionization continuing to occur in metal-enriched and therefore, biased regions in the Universe. 

Abstract The variations in Lyαforest opacity observed atz> 5.3 between lines of sight to different background quasars are too strong to be caused by fluctuations in the density field alone. The leading hypothesis for the cause of this excess variance is a late, ongoing reionization process at redshifts below six. Another model proposes strong ionizing background fluctuations coupled to a short, spatially varying mean free path of ionizing photons, without explicitly invoking incomplete reionization. With recent observations suggesting a short mean free path atz∼ 6, and a dramatic improvement inz> 5 Lyαforest data quality, we revisit this latter possibility. Here, we apply the likelihood-free inference technique of approximate Bayesian computation (ABC) to jointly constrain the hydrogen photoionization rate Γ_HIand the mean free path of ionizing photonsλ_mfpfrom the effective optical depth distributions atz= 5.0–6.1 from XQR-30. We find that the observations are well-described by fluctuating mean free path models with average mean free paths that are consistent with the steep trend implied by independent measurements atz∼ 5–6, with a concomitant rapid evolution of the photoionization rate. 

Abstract Luminous quasars are powerful targets to investigate the role of feedback from supermassive black holes (BHs) in regulating the growth phases of BHs themselves and of their host galaxies, up to the highest redshifts. Here we investigate the cosmic evolution of the occurrence and kinematics of BH-driven outflows, as traced by broad absorption line (BAL) features, due to the C iv ionic transition. We exploit a sample of 1935 quasars at z = 2.1–6.6 with bolometric luminosity log( L bol /erg s −1 ) ≳ 46.5, drawn from the Sloan Digital Sky Survey and from the X-Shooter legacy survey of Quasars at the Reionization Epoch (XQR-30). We consider rest-frame optical bright quasars to minimize observational biases due to quasar selection criteria. We apply a homogeneous BAL-identification analysis, based on employing composite template spectra to estimate the quasar intrinsic emission. We find a BAL quasar fraction close to 20% at z ∼ 2–4, while it increases to almost 50% at z ∼ 6. The velocity and width of the BAL features also increase at z ≳ 4.5. We exclude the possibility that the redshift evolution of the BAL properties is due to differences in terms of quasar luminosity and accretion rate. These results suggest significant BH feedback occurring in the 1 Gyr old universe, likely affecting the growth of BHs and, possibly, of their host galaxies, as supported by models of early BH and galaxy evolution. 

Abstract Measuring the density of the intergalactic medium using quasar sight lines in the epoch of reionization is challenging due to the saturation of Ly α absorption. Near a luminous quasar, however, the enhanced radiation creates a proximity zone observable in the quasar spectra where the Ly α absorption is not saturated. In this study, we use 10 high-resolution ( R ≳ 10,000) z ∼ 6 quasar spectra from the extended XQR-30 sample to measure the density field in the quasar proximity zones. We find a variety of environments within 3 pMpc distance from the quasars. We compare the observed density cumulative distribution function (CDF) with models from the Cosmic Reionization on Computers simulation and find a good agreement between 1.5 and 3 pMpc from the quasar. This region is far away from the quasar hosts and hence approaching the mean density of the universe, which allows us to use the CDF to set constraints on the cosmological parameter σ 8 = 0.6 ± 0.3. The uncertainty is mainly due to the limited number of high-quality quasar sight lines currently available. Utilizing the more than 200 known quasars at z ≳ 6, this method will allow us to tighten the constraint on σ 8 to the percent level in the future. In the region closer to the quasar within 1.5 pMpc, we find that the density is higher than predicted in the simulation by 1.23 ± 0.17, suggesting that the typical host dark matter halo mass of a bright quasar ( M 1450 < −26.5) at z ∼ 6 is log 10 ( M h / M ⊙ ) = 12.5 − 0.7 + 0.4 . 

ABSTRACT Recent quasar absorption line observations suggest that reionization may end as late as $$z \approx 5.3$$. As a means to search for large neutral hydrogen islands at $$z\ \lt\ 6$$, we revisit long dark gaps in the Ly $$\beta$$ forest in Very Large Telescope/X-Shooter and Keck/Echellette Spectrograph and Imager quasar spectra. We stack the Ly $$\alpha$$ forest corresponding to both edges of these Ly $$\beta$$ dark gaps and identify a damping wing-like extended absorption profile. The average redshift of the stacked forest is $z=5.8$. By comparing these observations with reionization simulations, we infer that such a damping wing-like feature can be naturally explained if these gaps are at least partially created by neutral islands. Conversely, simulated dark gaps lacking neutral hydrogen struggle to replicate the observed damping wing features. Furthermore, this damping wing-like profile implies that the volume-averaged neutral hydrogen fraction must be $$\langle x_{\rm H\,{\small {I}}} \rangle \ge 6.1 \pm 3.9~{{\ \rm per\ cent}}$$ at $z = 5.8$. Our results offer robust evidence that reionization extends below $z=6$. 

ABSTRACT Proximity zones of high-redshift quasars are unique probes of their central supermassive black holes as well as the intergalactic medium (IGM) in the last stages of reionization. We present 22 new measurements of proximity zones of quasars with redshifts between 5.8 and 6.6, using the enlarged XQR-30 sample of high-resolution, high-SNR quasar spectra. The quasars in our sample have ultraviolet magnitudes of M1450 ∼ −27 and black hole masses of 109–1010 M⊙. Our inferred proximity zone sizes are 2–7 physical Mpc, with a typical uncertainty of less than 0.5 physical Mpc, which, for the first time, also includes uncertainty in the quasar continuum. We find that the correlation between proximity zone sizes and the quasar redshift, luminosity, or black hole mass, indicates a large diversity of quasar lifetimes. Two of our proximity zone sizes are exceptionally small. The spectrum of one of these quasars, with z  = 6.02, displays, unusually for this redshift, damping wing absorption without any detectable metal lines, which could potentially originate from the IGM. The other quasar has a high-ionization absorber ∼0.5 pMpc from the edge of the proximity zone. This work increases the number of proximity zone measurements available in the last stages of cosmic reionization to 87. This data will lead to better constraints on quasar lifetimes and obscuration fractions at high redshift, that in turn will help probe the seed mass and formation redshift of supermassive black holes. 

Abstract The mean free path of ionizing photons,λ_mfp, is a critical parameter for modeling the intergalactic medium (IGM) both during and after reionization. We present direct measurements ofλ_mfpfrom QSO spectra over the redshift range 5 <z< 6, including the first measurements atz≃ 5.3 and 5.6. Our sample includes data from the XQR-30 VLT large program, as well as new Keck/ESI observations of QSOs nearz∼ 5.5, for which we also acquire new [Cii] 158μm redshifts with ALMA. By measuring the Lyman continuum transmission profile in stacked QSO spectra, we find ${\lambda }_{\mathrm{mfp}}={9.33}_{-1.80}^{+2.06}$, ${5.40}_{-1.40}^{+1.47}$, ${3.31}_{-1.34}^{+2.74}$, and ${0.81}_{-0.48}^{+0.73}$pMpc atz= 5.08, 5.31, 5.65, and 5.93, respectively. Our results demonstrate thatλ_mfpincreases steadily and rapidly with time over 5 <z< 6. Notably, we find thatλ_mfpdeviates significantly from predictions based on a fully ionized and relaxed IGM as late asz= 5.3. By comparing our results to model predictions and indirectλ_mfpconstraints based on IGM Lyαopacity, we find that the evolution ofλ_mfpis consistent with scenarios wherein the IGM is still undergoing reionization and/or retains large fluctuations in the ionizing UV background well below redshift 6. 

ABSTRACT The presence of excess scatter in the Ly-α forest at z ∼ 5.5, together with the existence of sporadic extended opaque Gunn-Peterson troughs, has started to provide robust evidence for a late end of hydrogen reionization. However, low data quality and systematic uncertainties complicate the use of Ly-α transmission as a precision probe of reionization’s end stages. In this paper, we assemble a sample of 67 quasar sightlines at z > 5.5 with high signal-to-noise ratios of >10 per ≤15 km s−1 spectral pixel, relying largely on the new XQR-30 quasar sample. XQR-30 is a large program on VLT/X-Shooter which obtained deep (SNR > 20 per pixel) spectra of 30 quasars at z > 5.7. We carefully account for systematics in continuum reconstruction, instrumentation, and contamination by damped Ly-α systems. We present improved measurements of the mean Ly-α transmission over 4.9 < z < 6.1. Using all known systematics in a forward modelling analysis, we find excellent agreement between the observed Ly-α transmission distributions and the homogeneous-UVB simulations Sherwood and Nyx up to z ≤ 5.2 (<1σ), and mild tension (∼2.5σ) at z = 5.3. Homogeneous UVB models are ruled out by excess Ly-α transmission scatter at z ≥ 5.4 with high confidence (>3.5σ). Our results indicate that reionization-related fluctuations, whether in the UVB, residual neutral hydrogen fraction, and/or IGM temperature, persist in the intergalactic medium until at least z = 5.3 (t = 1.1 Gyr after the big bang). This is further evidence for a late end to reionization. 

ABSTRACT The elemental abundances in the broad-line regions of high-redshift quasars trace the chemical evolution in the nuclear regions of massive galaxies in the early Universe. In this work, we study metallicity-sensitive broad emission-line flux ratios in rest-frame UV spectra of 25 high-redshift (5.8 < z < 7.5) quasars observed with the VLT/X-shooter and Gemini/GNIRS instruments, ranging over $$\log \left({{M}_{\rm {BH}}/\rm {M}_{\odot }}\right) = 8.4-9.8$$ in black hole mass and $$\log \left(\rm {L}_{\rm {bol}}/\rm {erg \, s}^{-1}\right) = 46.7-47.7$$ in bolometric luminosity. We fit individual spectra and composites generated by binning across quasar properties: bolometric luminosity, black hole mass, and blueshift of the C iv line, finding no redshift evolution in the emission-line ratios by comparing our high-redshift quasars to lower redshift (2.0 < z < 5.0) results presented in the literature. Using cloudy-based locally optimally emitting cloud photoionization model relations between metallicity and emission-line flux ratios, we find the observable properties of the broad emission lines to be consistent with emission from gas clouds with metallicity that are at least 2–4 times solar. Our high-redshift measurements also confirm that the blueshift of the C iv emission line is correlated with its equivalent width, which influences line ratios normalized against C iv. When accounting for the C iv blueshift, we find that the rest-frame UV emission-line flux ratios do not correlate appreciably with the black hole mass or bolometric luminosity.